periodic acid in water T=85°C; 0.333333 h; pH=7.1;

1: 96 percent / H5IO6 / H2O / 0.33 h / 85 °C / pH=7.1 2: 97 percent / tetrahydrofuran / 12 h / 25 °C View Scheme

1: 96 percent / H5IO6 / H2O / 0.33 h / 85 °C / pH=7.1 2: 97 percent / tetrahydrofuran / 12 h / 25 °C 3: 99 percent / H2, Et3N / 5percent Rh/C / ethanol / 30 h / 3040 Torr View Scheme