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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89220-93-9
合成路线
（共 14 条）
75-03-6
碘乙烷
+
6111-97-3
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反应条件
89220-93-9
+
89221-07-8
反应条件
sodium methylate in methanol 24 h; Heating;
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
536-74-3
苯乙炔
→
反应条件
89220-93-9
反应条件
1: 46.5 percent / 5.5percent HN3 / CHCl3 / 96 h / 120 °C 2: 85 percent / 18 M H2SO4, 13 M HNO3 / 1.5 h / 60 °C 3: 60 percent / sodium methoxide / methanol / 24 h / Heating View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
1680-44-0
4-苯基-1,2,3-三氮唑
→
反应条件
89220-93-9
反应条件
1: 85 percent / 18 M H2SO4, 13 M HNO3 / 1.5 h / 60 °C 2: 60 percent / sodium methoxide / methanol / 24 h / Heating View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-94-0
反应条件
hydrazine hydrate; palladium on activated charcoal in ethanol T=50°C;
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-95-1
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-96-2
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C 3: 94 percent / anhydrous K2CO3 / butan-2-one / 24 h / Heating View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-97-3
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C 3: 89 percent / anhydrous K2CO3 / butan-2-one / 24 h / Heating View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-98-4
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C 3: 94 percent / anhydrous K2CO3 / butan-2-one / 24 h / Heating 4: 83 percent / 1 M NaOH / ethanol / 0.75 h / 100 °C View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89220-99-5
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C 3: 89 percent / anhydrous K2CO3 / butan-2-one / 24 h / Heating 4: 82 percent / 1 M NaOH / ethanol / 0.75 h / 100 °C View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
89220-93-9
→
反应条件
89221-00-1
反应条件
1: 90 percent / 85percent hydrazine hydrate / 10percent Pd/C / ethanol / 50 °C 2: 91 percent / 18 M H2SO4, NaNO2 / H2O / 0 - 5 °C 3: 88 percent / anhydrous K2CO3 / 24 h / Heating View Scheme
参考文献
Livi; Biagi; Ferretti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 471 - 475
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