1: 94 percent / sodium iodide / acetone / 4 h / Heating
2: n-BuLi / tetrahydrofuran / 1 h / -78 - 25 °C / variation of nucleophile, time, temperature and solvent
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参考文献
Georg, Gunda; Durst, Tony
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2092 - 2095
n-butyllithium in tetrahydrofuran
T=-78 - 25°C; 1 h; variation of nucleophile, time and temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Georg, Gunda; Durst, Tony
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2092 - 2095