反应条件
1: 1.) aq. NaOH, 2.) K2S2O8, 4.) K2CO3
2: 1.) Mg, I2 / 1.) ether, reflux, 2 h, 2.) ether, reflux, 12 h
3: 84 percent / p-TsOH / benzene / 14 h / Heating
4: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 12 h / 760 Torr
5: 92 percent / BBr3 / CH2Cl2 / 12 h / 25 °C
View Scheme
参考文献
Singh, Udai S.; Scannell, Ralph T.; An, Haoyun; Carter, Barbara J.; Hecht, Sidney M.
Journal of the American Chemical Society, 1995 , vol. 117, # 51 p. 12691 - 12699
