反应条件
1: 1) Mg / 1) THF, reflux 0.5+1 h; 2) THF, -30 deg C, 10 min --> 0 deg C
2: 91 percent / nickel peroxide / diethyl ether / 0 deg C, 30 min --> r.t.
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参考文献
Jones, Todd K.; Denmark, Scott E.
Helvetica Chimica Acta, 1983 , vol. 66, # 8 p. 2377 - 2396
