2-溴-1-甲基-1H-吲哚合成路线 （共 3 条）
反应条件
methanol 1 h; Heating;
参考文献
Sako; Hirota; Maki
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3496 - 3502
反应条件
n-butyllithium; 1,2-dibromo-1,1,2,2-tetrachloroethane in tetrahydrofuran; hexane
T=-78 - 20°C; 1.16667 h;
参考文献
Miyamoto, Hiroshi; Hirano, Tomohiro; Okawa, Yoichiro; Nakazaki, Atsuo; Kobayashi, Susumu
Tetrahedron, 2013 , vol. 69, # 45 p. 9481 - 9493
反应条件
1: 62 percent / n-BuLi; I2 / diethyl ether; hexane / 1 h / 15 °C
2: 86 percent / n-BuLi; 1,2-dibromo-1,1,2,2-tetrachloroethane / tetrahydrofuran; hexane / 1.17 h / -78 - 20 °C
View Scheme
参考文献
Miyamoto, Hiroshi; Okawa, Yoichiro; Nakazaki, Atsuo; Kobayashi, Susumu
Angewandte Chemie - International Edition, 2006 , vol. 45, # 14 p. 2274 - 2277
