2-(甲基磺酰)苯磺酰氯化物合成路线 （共 13 条）
反应条件
chlorine in water; acetic acid Chlorination; oxidation;
参考文献
Langler, Richard Francis; Baerlocher, Felix J; Penn, Linda Z
Patent: US2003/220524 A1, 2003 ;
Location in patent: Page/Page column 26 ;
反应条件
hydrogenchloride; sulfur dioxide; acetic acid; sodium nitrite; copper(l) chloride in water
参考文献
Wyeth
Patent: US2003/109750 A1, 2003 ;
反应条件
potassium permanganate Erwaermen des Reaktionsprodukts mit PCl5 und POCl3;
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4783,4785
反应条件
chlorine; acetic acid in water T=-78 - 55°C; 8.5 h; Large scale reaction;
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
N-chloro-succinimide; acetic acid in water T=20 - 50°C; 4 h;
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
1: sodium periodate; RuCl3 monohydrate / dichloromethane; water; acetonitrile / 5 h / 50 °C / Large scale reaction 2: potassium hydroxide / N,N-dimethyl-formamide / 75 - 100 °C / Large scale reaction 3: chlorine; acetic acid / water / 8.5 h / -78 - 55 °C / Large scale reaction View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
1: potassium hydroxide / N,N-dimethyl-formamide / 60 - 100 °C / Large scale reaction 2: dihydrogen peroxide; acetic acid / water / 1 h / Reflux 3: potassium hydroxide / N,N-dimethyl-formamide / 75 - 100 °C / Large scale reaction 4: chlorine; acetic acid / water / 8.5 h / -78 - 55 °C / Large scale reaction View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
1: potassium hydroxide / N,N-dimethyl-formamide / 75 - 100 °C / Large scale reaction 2: chlorine; acetic acid / water / 8.5 h / -78 - 55 °C / Large scale reaction View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
1: sodium periodate; RuCl3 monohydrate / dichloromethane; water; acetonitrile / 5 h / 50 °C / Large scale reaction 2: potassium hydroxide / N,N-dimethyl-formamide / 75 - 100 °C / Large scale reaction 3: N-chloro-succinimide; acetic acid / water / 4 h / 20 - 50 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
反应条件
1: potassium hydroxide / N,N-dimethyl-formamide / 60 - 100 °C / Large scale reaction 2: dihydrogen peroxide; acetic acid / water / 1 h / Reflux 3: potassium hydroxide / N,N-dimethyl-formamide / 75 - 100 °C / Large scale reaction 4: N-chloro-succinimide; acetic acid / water / 4 h / 20 - 50 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 550 - 555
