(3beta)-3-羟基-2-(羟基亚氨基)齐墩果-12-烯-28-酸苯甲酯合成路线 （共 5 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran
T=0°C;
参考文献
Chen, Jun; Liu, Jun; Zhang, Luyong; Wu, Guanzhong; Hua, Weiyi; Wu, Xiaoming; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2915 - 2919
反应条件
1: 58 percent / NaNO2; aq. H2SO4 / methanol; tetrahydrofuran / 20 °C
2: 78 percent / NaBH4 / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chen, Jun; Liu, Jun; Zhang, Luyong; Wu, Guanzhong; Hua, Weiyi; Wu, Xiaoming; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2915 - 2919
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 60 °C
2: 89 percent / PCC / CH2Cl2 / 20 °C
3: 58 percent / NaNO2; aq. H2SO4 / methanol; tetrahydrofuran / 20 °C
4: 78 percent / NaBH4 / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chen, Jun; Liu, Jun; Zhang, Luyong; Wu, Guanzhong; Hua, Weiyi; Wu, Xiaoming; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2915 - 2919
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 60 °C
2: 89 percent / PCC / CH2Cl2 / 20 °C
3: 58 percent / NaNO2; aq. H2SO4 / methanol; tetrahydrofuran / 20 °C
4: 78 percent / NaBH4 / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chen, Jun; Liu, Jun; Zhang, Luyong; Wu, Guanzhong; Hua, Weiyi; Wu, Xiaoming; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2915 - 2919
反应条件
1: 89 percent / PCC / CH2Cl2 / 20 °C
2: 58 percent / NaNO2; aq. H2SO4 / methanol; tetrahydrofuran / 20 °C
3: 78 percent / NaBH4 / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chen, Jun; Liu, Jun; Zhang, Luyong; Wu, Guanzhong; Hua, Weiyi; Wu, Xiaoming; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2915 - 2919
