(5-甲氧基-2-硝基苯基)乙腈合成路线 （共 14 条）
反应条件
1: 33.5 g / 80percent sodium hydride / dimethylformamide / 3.5 h / 70 °C
2: 1 N Na2CO3 / 120 h / 40 °C
View Scheme
参考文献
Verboom; Lammerink; Egberink; et al.
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3797 - 3806
反应条件
1: hydroxylamine
2: acetic acid anhydride / 100 °C
View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1949 , p. 1074,1076
反应条件
2: carbon monoxide; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 72 h / 120 °C / 4560.31 Torr / Autoclave
View Scheme
参考文献
Banini, Serge R.; Turner, Michael R.; Cummings, Matthew M.; Soederberg, Bjoern C.G.
Tetrahedron, 2011 , vol. 67, # 20 p. 3603 - 3611
反应条件
1: 94 percent / anhydrous K2CO3, <18>crown-6 / acetonitrile / Heating
2: 38 percent / H2 / Pd/C (10percent Pd) / ethyl acetate / 3 h / 80 °C / 2280 Torr
View Scheme
参考文献
Makosza, Mieczyslaw; Danikiewicz, Witold; Wojciechowski, Krzysztof
Liebigs Annalen der Chemie, 1988 , p. 203 - 208
