反应条件
1: 77 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.5 h / Ambient temperature
2: 57 percent / toluene / 2 h / Heating
3: 0.1N NaHCO3, NaBH4 / 1 h
4: 33 percent / diethyl azodicarboxylate / CH2Cl2 / 1.) RT, 40 h, 2.) reflux, 1 h
View Scheme
参考文献
Heckel, Armin; Pfleiderer, Wolfgang
Tetrahedron Letters, 1983 , vol. 24, # 46 p. 5047 - 5050
