2,2,2-三氟-1-[4'-(甲基磺酰基)[1,1'-联苯]-4-基]乙酮合成路线 （共 3 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in water; isopropyl alcohol
T=110°C; Suzuki-Miyaura Coupling; 0.0833333 h; Microwave irradiation;
参考文献
De Oliveira Lopes, Raquel; De Miranda, Amanda S.; Reichart, Benedikt; Glasnov, Toma; Kappe, C. Oliver; Simon, Robert C.; Kroutil, Wolfgang; Miranda, Leandro S.M.; Leal, Ivana C.R.; De Souza, Rodrigo O.M.A.
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 104, p. 101 - 107
反应条件
dihydrogen peroxide; sodium tungstate; tetra(n-butyl)ammonium hydrogensulfate in tetrahydrofuran; water; toluene
T=45 - 59°C; 3.5 h; Title compound not separated from byproducts;
参考文献
Dolman, Sarah J.; Gosselin, Francis; O'Shea, Paul D.; Davies, Ian W.
Tetrahedron, 2006 , vol. 62, # 21 p. 5092 - 5098
反应条件
in toluene
1 h; Heating;
参考文献
Dolman, Sarah J.; Gosselin, Francis; O'Shea, Paul D.; Davies, Ian W.
Tetrahedron, 2006 , vol. 62, # 21 p. 5092 - 5098
