反应条件
1: (+/-)-cyclohexanone-4-carboxaldehyde With n-butyllithium; trimethylaluminum; O,N-dimethyl-hydroxylamine hydrochloride in tetrahydrofuran; hexane
T=0 - 20°C; 2 h;
2: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane
T=0 - 20°C; Wittig Olefination; 4 h;
参考文献
Barrios, Francis J.; Springer, Brannon C.; Colby, David A.
Organic Letters, 2013 , vol. 15, # 12 p. 3082 - 3085
