反应条件
1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C 2.) THF, hexane, 0 deg C
2: 1.) n-butyllithium, HMPA / 1.)THF, hexane, -78 degC to 0 degC 2.) 45-50 degC, 2 h
3: 63 percent / 5percent HCl / tetrahydrofuran; H2O / 2 h / 50 °C
View Scheme
参考文献
Sternberg; Vollhardt
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1574 - 1583
