3-chloro-benzenecarboperoxoic acid in chloroform 10 h; Ambient temperature;

1: 23 percent / 1.) conc. H2SO4 / acetic acid / 1.) 80 deg C, 2 h, 2.) room temp., 1 h 2: 52 percent / m-chloroperbenzoic acid / CHCl3 / 10 h / Ambient temperature View Scheme

1: 23 percent / 1.) conc. H2SO4 / acetic acid / 1.) 80 deg C, 2 h, 2.) room temp., 1 h 2: 52 percent / m-chloroperbenzoic acid / CHCl3 / 10 h / Ambient temperature View Scheme