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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89441-55-4
合成路线
（共 7 条）
66-99-9
2-萘甲醛
+
89467-10-7
→
反应条件
89441-55-4
反应条件
sodium hydride in dimethyl sulfoxide T=80°C; 24 h;
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
81-84-5
萘酐
→
反应条件
89441-55-4
反应条件
1: 60 percent / KMnO4 2: 73 percent / Ra-Ni / 250 °C 3: 92 percent / H2SO4 / benzene 4: 95 percent / LiAlH4 / diethyl ether / 3 h / Heating 5: 88 percent / 48 percent HBr / 1 h / 50 °C 6: 93 percent / xylene / 2 h / Heating 7: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
3112-43-4
→
反应条件
89441-55-4
反应条件
1: 73 percent / Ra-Ni / 250 °C 2: 92 percent / H2SO4 / benzene 3: 95 percent / LiAlH4 / diethyl ether / 3 h / Heating 4: 88 percent / 48 percent HBr / 1 h / 50 °C 5: 93 percent / xylene / 2 h / Heating 6: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
83-32-9
苊
→
反应条件
89441-55-4
反应条件
1: 92 percent / sodium bichromate 2: 60 percent / KMnO4 3: 73 percent / Ra-Ni / 250 °C 4: 92 percent / H2SO4 / benzene 5: 95 percent / LiAlH4 / diethyl ether / 3 h / Heating 6: 88 percent / 48 percent HBr / 1 h / 50 °C 7: 93 percent / xylene / 2 h / Heating 8: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
41563-68-2
→
反应条件
89441-55-4
反应条件
1: 93 percent / xylene / 2 h / Heating 2: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
51689-51-1
→
反应条件
89441-55-4
反应条件
1: 88 percent / 48 percent HBr / 1 h / 50 °C 2: 93 percent / xylene / 2 h / Heating 3: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
28269-31-0
2-甲基异邻苯二甲酸二甲酯
→
反应条件
89441-55-4
反应条件
1: 95 percent / LiAlH4 / diethyl ether / 3 h / Heating 2: 88 percent / 48 percent HBr / 1 h / 50 °C 3: 93 percent / xylene / 2 h / Heating 4: 77 percent / NaH / dimethylsulfoxide / 24 h / 80 °C View Scheme
参考文献
Brison, Jean; Bakker, Claude de; Defay, Nicole; Geerts-Evrard, France; Marchant, Marie-Jeanne; Martin, Richard H.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 10 p. 901 - 912
