4-溴-2-氯-1-硝基苯合成路线 (共 3 条)
反应条件
sodium tert-pentoxide; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=100°C; 3 h;
参考文献
LABORATORIOS DEL DR. ESTEVE, S.A.
Patent: WO2006/69807 A1, 2006 ;
Location in patent: Page/Page column 104 ;
WO 2006/069807 A1
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=100°C; 4 h;
参考文献
Tasler, Stefan; Mies, Jan; Lang, Martin
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2286 - 2300
反应条件
ethanol; iron; calcium chloride in water T=60°C; 0.416667 h; chemoselective reaction;
参考文献
Chandrappa; Vinaya; Ramakrishnappa; Rangappa
Synlett, 2010 , # 20 art. no. D13110ST, p. 3019 - 3022