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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89523-62-6
合成路线
(共 16 条)
141-30-0
3,6-二氯哒嗪
+
89523-62-6
→
反应条件
34102-86-8
+
58059-29-3
3-氯-6-(4-氯苯基)-哒嗪
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 24 h;
参考文献
Chekmarev, Dmitriy S.; Stepanov, Alexander E.; Kasatkin, Alexander N.
Tetrahedron Letters, 2005 , vol. 46, # 8 p. 1303 - 1305
1041479-70-2
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
+
14310-22-6
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
89523-62-6
→
反应条件
14310-22-6
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1205517-06-1
+
89523-62-6
→
反应条件
14310-22-6
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1205517-07-2
+
89523-62-6
→
反应条件
14310-22-6
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
+
14310-22-6
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 630 - 634
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
反应条件
bis(acetylacetonate)nickel(II); 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=-10°C; Negishi type coupling; Inert atmosphere; Kinetics;
参考文献
Journal of the American Chemical Society, , vol. 131, # 29 p. 9892 - 9893
149683-48-7
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
+
91335-74-9
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 630 - 634
1041479-71-3
+
89523-62-6
→
反应条件
2050-68-2
4,4'-二氯联苯
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 630 - 634
1041479-72-4
+
89523-62-6
→
反应条件
1205517-10-7
+
2050-68-2
4,4'-二氯联苯
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 630 - 634
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