4-甲酰基-1H-咪唑-1-羧酸 1,1-二甲基乙酯合成路线 (共 3 条)
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
参考文献
Bristol-Myers Squibb Company
Patent: US6011029 A1, 2000 ;
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Schering Aktiengesellschaft
Patent: US2005/90541 A1, 2005 ;
Location in patent: Page/Page column 31-32 ;
反应条件
oxalyl dichloride; dimethyl sulfoxide in dichloromethane
T=-78°C; 0.25 h;
参考文献
Kimura, Rumi; Nagano, Tanemasa; Kinoshita, Hideki
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 11 p. 2517 - 2525