1: 0.62 g / sodium hydroxide / various solvent(s) / 1 h / 75 °C
2: 0.12 g / benzene / 2 h / 190 °C / pyrolysis, in sealed tube
3: 0.095 g / methanol / 12 h
View Scheme
参考文献
Dodsworth, D. J.; Jenkins, C. M.; Stephens, R.; Tatlow, J. C.
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 41 - 60
1: 1.1 g / NaBH4 / bis-(2-methoxy-ethyl) ether / 1.67 h / -5 °C
2: 0.62 g / sodium hydroxide / various solvent(s) / 1 h / 75 °C
3: 0.12 g / benzene / 2 h / 190 °C / pyrolysis, in sealed tube
4: 0.095 g / methanol / 12 h
View Scheme
参考文献
Dodsworth, D. J.; Jenkins, C. M.; Stephens, R.; Tatlow, J. C.
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 41 - 60
1: 1.) CoF3; 2.) KOH / 1.) 160-170 deg C; 2.) water, reflux, 24 h
2: 1.1 g / NaBH4 / bis-(2-methoxy-ethyl) ether / 1.67 h / -5 °C
3: 0.62 g / sodium hydroxide / various solvent(s) / 1 h / 75 °C
4: 0.12 g / benzene / 2 h / 190 °C / pyrolysis, in sealed tube
5: 0.095 g / methanol / 12 h
View Scheme
参考文献
Dodsworth, D. J.; Jenkins, C. M.; Stephens, R.; Tatlow, J. C.
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 41 - 60
