sodium azide in N,N-dimethyl-formamide
T=60°C; 5 h;
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
1: 70 percent / acetonitrile / 72 h / Ambient temperature
2: 83 mg / dimethylsulfoxide / 0.03 h / Heating
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
1: 70 percent / acetonitrile / 72 h / Ambient temperature
2: HCl gas
3: 35 percent / NaN3 / dimethylformamide / 0.08 h / 60 °C
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137