4-羟基-5-苯基-3(2H)-异噻唑酮 1,1-二氧化物合成路线 （共 4 条）
反应条件
sodium t-butanolate in tert-butyl alcohol
T=40 - 45°C; Cyclization; 2.5 h;
参考文献
Zlotin, S. G.; Gerasyuto, A. I.
Russian Chemical Bulletin, 1999 , vol. 48, # 2 p. 394 - 395
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1999 , # 2 p. 396 - 398
反应条件
sodium t-butanolate in tert-butyl alcohol
T=40°C; Cycloaddition; 2 h;
参考文献
Zlotin, S. G.; Gerasyuto, A. I.
Russian Chemical Bulletin, 1999 , vol. 48, # 2 p. 394 - 395
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1999 , # 2 p. 396 - 398
反应条件
hydrogenchloride
1 h;
参考文献
Rooney, C. S.; Cochran, D. W.; Ziegler, C.; Cragoe, E. J.; Williams, H. W. R.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2212 - 2217
反应条件
1: 57 percent / MeONa / methanol / 6 h / 20 °C
2: 55 percent / t-BuONa / 2-methyl-propan-2-ol / 2.5 h / 40 - 45 °C
View Scheme
参考文献
Zlotin, S. G.; Gerasyuto, A. I.
Russian Chemical Bulletin, 1999 , vol. 48, # 2 p. 394 - 395
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1999 , # 2 p. 396 - 398
