trifluoroacetic acid in 1,2-dichloro-ethane 4 h; Heating;

1: 69 percent / ClSCN / acetic acid / 0.5 h / Ambient temperature 2: 94 percent / 1N NaOH / 2-methyl-propan-2-ol / 2.5 h / Ambient temperature 3: 96 percent / 2N NaOH / ethanol / 1 h / Ambient temperature 4: 83 percent / trifluoroacetic acid / 1,2-dichloro-ethane / 4 h / Heating View Scheme

1: 94 percent / 1N NaOH / 2-methyl-propan-2-ol / 2.5 h / Ambient temperature 2: 96 percent / 2N NaOH / ethanol / 1 h / Ambient temperature 3: 83 percent / trifluoroacetic acid / 1,2-dichloro-ethane / 4 h / Heating View Scheme

1: 96 percent / 2N NaOH / ethanol / 1 h / Ambient temperature 2: 83 percent / trifluoroacetic acid / 1,2-dichloro-ethane / 4 h / Heating View Scheme