4-(Boc-氨基甲基)异硫氰酸苯酯合成路线 （共 4 条）
反应条件
calcium carbonate in chloroform; water
T=20°C; 16 h;
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
反应条件
1: 91 percent / Et3N / CH2Cl2 / 16 h / 0 °C
2: 31 percent / SnCl2*2H2O / ethanol / 1 h / Heating
3: 26 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
反应条件
1: 91 percent / Et3N / CH2Cl2 / 16 h / 0 °C
2: 31 percent / SnCl2*2H2O / ethanol / 1 h / Heating
3: 26 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
反应条件
1: 31 percent / SnCl2*2H2O / ethanol / 1 h / Heating
2: 26 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
