反应条件
1: 1.) MeMgI / 1.) diethyl ether, reflux, 30 min, 2.) diethyl ether, reflux, 1 h
2: 75 percent / potassium hydroxide, hydrazine hydrate / ethane-1,2-diol / 3.5 h / Heating
3: phosphorus oxychloride / diethyl ether
4: sodium hydroxide / H2O
View Scheme
参考文献
Bowden, Bruce F.; Clezy, Peter S.; Coll, John C.; Ravi, B. N.; Tapiolas, Dianne M.
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 227 - 230