反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '7240612', constants.ctx, '0')">Bu<sub>4</sub>N[Fe(CO)3(NO)]</a>; <a href="#" onclick="return RXDsubstances(event, this, '957171', constants.ctx, '0')">tri-cyclo-hexyl-phosphine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102551', constants.ctx, '0')">1,4-dioxane</a> <br />T=50°C; Inert atmosphere; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>; <a href="#" onclick="return RXDsubstances(event, this, '8128150', constants.ctx, '0')">sodium hydroxide</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102551', constants.ctx, '0')">1,4-dioxane</a>; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a> <br />T=20°C; 1.5 h; Inert atmosphere; chemoselective reaction; <br />
参考文献
Dieskau, Andre P.; Begouin, Jeanne-Marie; Plietker, Bernd European Journal of Organic Chemistry, 2011 , # 27 p. 5291 - 5296