雄甾-1,4-二烯-3,17-二酮合成路线 (共 75 条)
反应条件
potassium tert-butylate in tert-butyl alcohol 20 h;
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 6 p. 788 - 795
反应条件
1: dibenzoyl peroxide; CCl4; N-bromo-succinimide 2: 2,4,6-trimethyl-pyridine 3: glass / 600 °C View Scheme
参考文献
Kaufmann et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4531,4533
反应条件
1: 20 h / Heating 2: 1.10 g / benzene; ethanol; H2O / 5 h / 20 °C View Scheme
参考文献
Buzzetti; Di Salle; Longo; Briatico
Steroids, 1993 , vol. 58, # 11 p. 527 - 532
反应条件
1: pyridine; hydrogen sulfide; sulfur
2: NaBH4
View Scheme
参考文献
Tweit; Dodson
Journal of the American Chemical Society, 1959 , vol. 81, p. 4409,4411
反应条件
in hexane; methyl acetate; water
参考文献
Schering Aktiengesellschaft
Patent: US5523428 A1, 1996 ;