sodium hydrogencarbonate in ethyl acetate Ambient temperature;

1: 6.9 g / hydrogen / 10percent Pd-C / acetic acid / Ambient temperature; Parr apparatus 2: 93 percent / thionyl chloride / 1.) 50 deg C, 4 h, 2.) room temperature, 48 h 3: 88 percent / 1 M NaHCO3 / ethyl acetate / Ambient temperature View Scheme

1: 93 percent / thionyl chloride / 1.) 50 deg C, 4 h, 2.) room temperature, 48 h 2: 88 percent / 1 M NaHCO3 / ethyl acetate / Ambient temperature View Scheme