6-氨基-3-苯基-1,2,4-三嗪-5(2H)-硫酮合成路线 （共 11 条）
反应条件
tetraphosphorus decasulfide in 1,4-dioxane
1.5 h; Heating;
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
1: 79 percent / methanol / 72 h
2: 80 percent / P2S5 / dioxane / 1.5 h / Heating
View Scheme
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
hydrazine in ethanol
3 h; Heating;
参考文献
Neunhoeffer; Dostert; Hammann
Synthesis, 1988 , # 10 p. 778 - 782
反应条件
sodium hydroxide in water
1 h; Ambient temperature;
参考文献
Jacobsen, Noel W.; Philippides, Athena E.
Australian Journal of Chemistry, 1987 , vol. 40, # 3 p. 491 - 499
反应条件
sodium hydroxide in water
72 h;
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
1: 56 percent / 2 N NaOH / H2O / 72 h
2: 98 percent / 12 h / Ambient temperature
3: 58 percent / P2S5 / dioxane / 1 h / Heating
View Scheme
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
T=70°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
T=70°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
1: 56 percent / 2 N NaOH / H2O / 72 h
2: 98 percent / 12 h / Ambient temperature
View Scheme
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
反应条件
1: 56 percent / 2 N NaOH / H2O / 72 h
2: 1) ethyl chloroformiate; 2) H2NNH2 / 1) diethylenglycol dimethyl ether, 24 h; 2) C2H5OH, 2 h, reflux
View Scheme
参考文献
Neunhoeffer, Hans; Hammann, Heinz
Liebigs Annalen der Chemie, 1984 , # 2 p. 283 - 295
