反应条件
1: 6-Bromoquinoline With 1,10-phenanthroline; K2S2O5; tetrabutylammomium bromide; sodium formate; palladium diacetate; triphenylphosphine in dimethyl sulfoxide
T=70°C; 20 h; Inert atmosphereMicrowave irradiation;
2: methyl iodide in dimethyl sulfoxide
T=23°C; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Shavnya, Andrei; Coffey, Steven B.; Smith, Aaron C.; Mascitti, Vincent
Organic Letters, 2013 , vol. 15, # 24 p. 6226 - 6229