2-甲基-6-(甲基磺酰基)吡啶-3-胺合成路线 （共 3 条）
反应条件
(CuOTf)2.C6H6; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide
T=150°C; 4 h;
参考文献
Erickson, Shawn David; Gillespie, Paul; Guertin, Kevin Richard; Karnachi, Prabha Saba; Kim, Kyungjin; Ma, Chun; McComas, Warren William; Pietranico-Cole, Sherrie Lynn; Qi, Lida; Tilley, Jefferson Wright; Zhang, Qiang
Patent: US2009/286812 A1, 2009 ;
Location in patent: Page/Page column 19 ;
反应条件
methanesulfinic acid sodium salt; (CuOTf)2.C6H6; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide
T=150°C; 4 h; Product distribution / selectivity;
参考文献
ARENA PHARMACEUTICALS, INC.
Patent: WO2008/5576 A1, 2008 ;
Location in patent: Page/Page column 28 ;
反应条件
ammonium chloride; zinc in water; ethyl acetate
T=0 - 20°C; 17 h; Product distribution / selectivity;
参考文献
ARENA PHARMACEUTICALS, INC.
Patent: WO2008/5576 A1, 2008 ;
Location in patent: Page/Page column 29 ;
