in hexane
addn. of hexane and phenylazide to tert-butyl(tert-butylimino)borane at0°C, stirring at 50°C for 5h; removal of all volatile components and excess of phenylazide, elem.anal.;
参考文献
Paetzold, Peter; Plotho, Christoph von; Guenter, Schmid; Boese, Roland; Schrader, Bernhard; et al.
Chemische Berichte, 1984 , vol. 117, p. 1089 - 1102
azidotrimethylsilane
addn. of tert-butyl(tert-butylimino)borane to azidotrimethylsilane at 0°C, stirring at room temp. for 2h; removal of all volatile components, elem.anal.;
参考文献
Paetzold, Peter; Plotho, Christoph von; Guenter, Schmid; Boese, Roland; Schrader, Bernhard; et al.
Chemische Berichte, 1984 , vol. 117, p. 1089 - 1102
