3-(4-丁氧基苯基)丙酰肼合成路线 (共 3 条)
反应条件
hydrazine hydrate
T=100°C; 2 h; Yield given;
参考文献
Freudenreich, Charles; Samama, Jean-Pierre; Biellmann, Jean-Francois
Journal of the American Chemical Society, 1984 , vol. 106, # 11 p. 3344 - 3353
反应条件
1: 1.) KOH; 2.) 13 N KOH / 1.) MeOH, reflux, 8 h; 2.) H2O, reflux, 1.5 h
2: HCl / 1 h / Heating
3: hydrazin hydrate / 2 h / 100 °C
View Scheme
参考文献
Freudenreich, Charles; Samama, Jean-Pierre; Biellmann, Jean-Francois
Journal of the American Chemical Society, 1984 , vol. 106, # 11 p. 3344 - 3353
反应条件
1: HCl / 1 h / Heating
2: hydrazin hydrate / 2 h / 100 °C
View Scheme
参考文献
Freudenreich, Charles; Samama, Jean-Pierre; Biellmann, Jean-Francois
Journal of the American Chemical Society, 1984 , vol. 106, # 11 p. 3344 - 3353