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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89806-04-2
合成路线
（共 9 条）
141-52-6
乙醇钠
+
89806-04-2
→
反应条件
111854-29-6
反应条件
in ethanol 1 h; Ambient temperature;
参考文献
Toyooka, Kouhei; Kawashima, Yasushi; Kubota, Seiju
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 3 p. 1030 - 1035
89806-03-1
→
反应条件
89806-04-2
反应条件
dihydrogen peroxide in acetic acid T=90°C; 2.5 h;
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
39577-51-0
→
反应条件
89806-04-2
反应条件
dihydrogen peroxide in acetic acid T=70°C; 1 h;
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
39577-53-2
→
反应条件
39577-51-0
+
89806-04-2
反应条件
dihydrogen peroxide in acetic acid T=50°C; 5 h;
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
26152-32-9
→
反应条件
89806-04-2
反应条件
dihydrogen peroxide; acetic anhydride 1.) 90 deg C, 1 h, 2.) H2O, 90 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
89806-15-5
→
反应条件
89806-04-2
反应条件
1: 3 percent / 30percent H2O2 / acetic acid / 38 h / Ambient temperature 2: 78 percent / 30percent H2O2 / acetic acid / 1 h / 70 °C View Scheme
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
89806-20-2
→
反应条件
89806-04-2
反应条件
1: 77 percent / m-chloroperbenzoic acid / CHCl3 / 2.5 h / 0 °C 2: 50 percent / 30percent H2O2 / acetic acid / 5 h / 50 °C 3: 78 percent / 30percent H2O2 / acetic acid / 1 h / 70 °C View Scheme
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
89806-17-7
→
反应条件
89806-04-2
反应条件
1: 24 percent / 30percent H2O2 / acetic acid / 48 h 2: 78 percent / 30percent H2O2 / acetic acid / 1 h / 70 °C View Scheme
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
39577-53-2
→
反应条件
89806-04-2
反应条件
1: 50 percent / 30percent H2O2 / acetic acid / 5 h / 50 °C 2: 78 percent / 30percent H2O2 / acetic acid / 1 h / 70 °C View Scheme
参考文献
Kubota, Seiju; Toyooka, Kouhei; Misra, Hemant K.; Kawano, Michinobu; Shibuya, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2957 - 2962
