6-氰基吡啶-3-甲酸甲酯合成路线 (共 8 条)
反应条件
in methanol; diethyl ether T=0 - 20°C; 2 h;
参考文献
Dublanchet, Anne-Claude; Compere, Delphine; Cluzeau, Philippe; Blais, Stephane; Denis, Alexis; Ducrot, Pierre; Courte, Karine; Descamps, Sophie
Patent: US2004/72871 A1, 2004 ;
Location in patent: Page/Page column 23 ;
反应条件
potassium carbonate in acetone
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane 2.16667 h;
参考文献
EP2154135 A1, ;
Page/Page column 20 ;
反应条件
in acetonitrile T=27°C; Yield given. Yields of byproduct given;
参考文献
Heterocycles, , vol. 22, # 5 p. 1121 - 1124
反应条件
in acetonitrile T=27°C; Yield given. Yields of byproduct given;
参考文献
Heterocycles, , vol. 22, # 5 p. 1121 - 1124
反应条件
N,N-dimethylcarbamoyl chloride in dichloromethane Ambient temperatureother 3-substituted pyridine 1-oxides, var. temps.; Product distributionMechanism;
参考文献
Heterocycles, , vol. 22, # 1 p. 93 - 96
反应条件
methanol; sodium tetrahydroborate in tetrahydrofuran
T=20°C; Cooling with ice;
参考文献
Mitsubishi Tanabe Pharma Corporation
Patent: EP2154135 A1, 2010 ;
Location in patent: Page/Page column 20; 21 ;