sodium iodide in acetonitrile Heating; Yield given;

1: NaI / acetonitrile / Heating 2: 25 percent Chromat. / tetraethylammonium iodide, 1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane nickel(II) perchlorate / dimethylformamide / Ambient temperature; electrolysis View Scheme

1: NaI / acetonitrile / Heating 2: 34 percent Chromat. / tetraethylammonium iodide, 1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane nickel(II) perchlorate / dimethylformamide / Ambient temperature; electrolysis View Scheme