1: (dimethyl)-methyl phosphonate With n-butyllithium in diethyl ether; hexane
T=-78°C; 0.5 h;
2: isovaleraldehyde in diethyl ether
1 h;
3: With sulfuric acid in diethyl ether
0.166667 h; Further stages.;
参考文献
Woschek; Lindner, Wolfgang; Hammerschmidt
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 12 p. 1287 - 1298