4-(3,3-二甲基丁酰基)苯甲腈合成路线 (共 2 条)
反应条件
SPB in tetrahydrofuran; water T=20°C; Inert atmosphere;
参考文献
Kim, Hye Ryung; Yun, Jaesook
Chemical Communications, 2011 , vol. 47, # 10 p. 2943 - 2945
反应条件
1: para-bromobenzonitrile With magnesium; lithium chloride in tetrahydrofuran T=25°C; 0.75 h; Inert atmosphere; 2: With CCl2CuN(2-)*2Li(1+) in tetrahydrofuran T=-20°C; 0.5 h; Inert atmosphere; 3: 3,3-dimethylbutanoyl chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 29 p. 7192 - 7202