1-(3-甲氧基苯基)-3-(4-甲氧基苯基)-1-丙酮合成路线 （共 9 条）
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in toluene
T=80°C; 24 h; Inert atmosphere;
参考文献
Ramulu, B. Venkat; Mahendar; Krishna; Reddy, A. Gopi Krishna; Suchand; Satyanarayana
Tetrahedron, 2013 , vol. 69, # 38 p. 8305 - 8315
反应条件
(2-phenylphenyl)diphenylphosphane; palladium diacetate; caesium carbonate in toluene
T=80°C; 24 h; Inert atmosphere;
参考文献
Ramulu, B. Venkat; Mahendar; Krishna; Reddy, A. Gopi Krishna; Suchand; Satyanarayana
Tetrahedron, 2013 , vol. 69, # 38 p. 8305 - 8315
反应条件
cesium fluoride in toluene; acetonitrile
T=75°C; Diels-Alder reaction; 60.5 h;
参考文献
Zhang, Tiexin; Huang, Xian; Wu, Luling
European Journal of Organic Chemistry, 2012 , # 18 p. 3507 - 3519
反应条件
1.1: palladium diacetate; triethylamine / acetonitrile / 24 h / 80 °C / Inert atmosphere
2.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: palladium diacetate; caesium carbonate; triphenylphosphine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
反应条件
1.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: palladium diacetate; caesium carbonate; triphenylphosphine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
反应条件
1.1: palladium diacetate; triethylamine / acetonitrile / 24 h / 80 °C / Inert atmosphere
2.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: palladium diacetate; caesium carbonate; triphenylphosphine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
反应条件
1.1: palladium diacetate; triethylamine / acetonitrile / 24 h / 80 °C / Inert atmosphere
2.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: potassium tert-butylate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
反应条件
1.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: potassium tert-butylate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
反应条件
1.1: palladium diacetate; triethylamine / acetonitrile / 24 h / 80 °C / Inert atmosphere
2.1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: potassium tert-butylate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine / toluene / 24 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Suchand; Krishna; Venkat Ramulu; Dibyendu; Gopi Krishna Reddy; Mahendar; Satyanarayana
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3861 - 3864
