联锡酰氨基己酰-6-氨基己酸N-羟基琥珀酰亚胺酯合成路线 （共 3 条）
反应条件
in N,N-dimethyl-formamide T=-5°C; 1.83333 h;
参考文献
US2012/232262 A1, ;
Page/Page column 3 ;
反应条件
1.1: triethylamine / 1-methyl-pyrrolidin-2-one / 2 h / 60 °C 2.1: 1-methyl-pyrrolidin-2-one / 50 - 100 °C 3.1: triethylamine / N,N-dimethyl-formamide / 0.25 h / -5 °C 3.2: 3 h / -5 °C 4.1: N,N-dimethyl-formamide / 1.83 h / -5 °C View Scheme
反应条件
1.1: 1-methyl-pyrrolidin-2-one / 50 - 100 °C 2.1: triethylamine / N,N-dimethyl-formamide / 0.25 h / -5 °C 2.2: 3 h / -5 °C 3.1: N,N-dimethyl-formamide / 1.83 h / -5 °C View Scheme
