2-氯-6-甲基苯甲酰氯合成路线 （共 13 条）
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, CuSO4, aq. NH3, benzene
2: aq. KOH / ethanol / Heating
3: aq. NaNO2, H2SO4
4: SOCl2
View Scheme
参考文献
Haering,M.
Helvetica Chimica Acta, 1960 , vol. 43, p. 104 - 113
反应条件
1: aq. NaNO2, H2SO4
2: SOCl2
View Scheme
参考文献
Haering,M.
Helvetica Chimica Acta, 1960 , vol. 43, p. 104 - 113
反应条件
1: in dichloromethane
T=0°C; 0.75 h;
2: With triethylamine
T=20°C;
参考文献
X-CEPTOR THERAPEUTICS, INC.; SANKYO COMPANY, LIMITED
Patent: WO2004/58717 A1, 2004 ;
Location in patent: Page 76 ;
WO 2004/058717 A1
