4-氰基-[1,1-联苯]-4-羧酸甲酯合成路线 （共 15 条）
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Tetrahedron, , vol. 58, # 42 p. 8417 - 8424
反应条件
in N,N-dimethyl-formamide T=130°C; 16 h;
参考文献
Fletcher, David I.; Ganellin, C. Robin; Piergentili, Alessandro; Dunn, Philip M.; Jenkinson, Donald H.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 16 p. 5457 - 5479
反应条件
sodium methylate; caesium carbonate; potassium iodide; Merrifield resin; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride 1.) DMF, 80 deg C, 18 h; 2.) THF, r.t., 18 h; 3.) THF, 70 deg C, 18 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 31 p. 5491 - 5494
反应条件
sulfuric acid 6 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 1 p. 35 - 38
反应条件
water in methanol T=30 - 50°C; ΔH(excit), ΔS(excit), log A; Rate constantThermodynamic dataKinetics;
参考文献
Ananthakrishnanadar, Ponnambalanad.; Kannan, Nagarathnam
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 1 p. 35 - 38
