4-(4-氯苯基)苯甲酸甲酯合成路线 (共 8 条)
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; potassium carbonate; PdI2 in water; isopropyl alcohol T=80°C; Suzuki reaction; 5 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
tetrakis(triphenylphosphine) palladium(0) T=80°C; Stille cross-coupling; 17 h; Ionic liquidInert atmosphere;
参考文献
Hao, Wenyan; Xi, Zhiwen; Cai, Mingzhong
Synthetic Communications, 2012 , vol. 42, # 16 p. 2396 - 2406
反应条件
palladium on activated charcoal in m-xylene T=140°C; 10 h;
参考文献
Matsushita; Sakamoto; Murakami; Matsui
Synthetic Communications, 1994 , vol. 24, # 22 p. 3307 - 3313
反应条件
1: C14H10ClO2Pol With trifluoroacetic acid in dichloromethane T=20°C; 0.833333 h; Wang resin; 2: diazomethane
参考文献
ACS Combinatorial Science, , vol. 16, # 5 p. 211 - 214
参考文献
Journal of the American Chemical Society, , vol. 76, p. 4543,4544
反应条件
sulfuric acid 6 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 1 p. 35 - 38
反应条件
Yield given. Multistep reaction;
参考文献
Synlett, , # 3 p. 295 - 297
反应条件
water in methanol T=30 - 50°C; ΔH(excit), ΔS(excit), log A; Rate constantThermodynamic dataKinetics;
参考文献
Ananthakrishnanadar, Ponnambalanad.; Kannan, Nagarathnam
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 1 p. 35 - 38