triethylamine; trichlorophosphate in dichloromethane
T=-20°C; 3.5 h;
参考文献
Eijk, J. M. van der; Richters, V. E. M.; Nolte, R. J. M.; Drenth, W.
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 1 p. 46 - 50
1: dimethylformamide / Ambient temperature
2: formic acid / 1 h
3: 40 percent / triethylamine, POCl3 / CH2Cl2 / 3.5 h / -20 °C
View Scheme
参考文献
Eijk, J. M. van der; Richters, V. E. M.; Nolte, R. J. M.; Drenth, W.
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 1 p. 46 - 50
1: dimethylformamide / Ambient temperature
2: formic acid / 1 h
3: 40 percent / triethylamine, POCl3 / CH2Cl2 / 3.5 h / -20 °C
View Scheme
参考文献
Eijk, J. M. van der; Richters, V. E. M.; Nolte, R. J. M.; Drenth, W.
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 1 p. 46 - 50
