N-苯甲酰基-beta-丙氨酸甲酯合成路线 (共 7 条)
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=60°C; 11 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 29, # 6 p. 635 - 641
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 743 - 750
参考文献
Xu, Hongyu; Jia, Li
Organic Letters, 2003 , vol. 5, # 9 p. 1575 - 1577
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
参考文献
Bahde, Robert J.; Appella, Daniel H.; Trenkle, William C.
Tetrahedron Letters, 2011 , vol. 52, # 32 p. 4103 - 4105
反应条件
1: 92 percent / BnCo(CO)4; (BnCO)Co(CO)4 / hexane; tetrahydrofuran / 48 h / 60 °C / 10343 Torr 2: 80 percent / 24 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 5, # 9 p. 1575 - 1577
反应条件
1.1: sodium hydrogencarbonate / water 1.2: 1.5 h / 0 - 20 °C 2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 32 p. 4103 - 4105
参考文献
Yakugaku Zasshi, , vol. 71, p. 1007
Chem.Abstr., , p. 8121
反应条件
N-bromosuccinmide; potassium carbonate in 1,2-dichloro-ethane T=100°C; 36 h;
参考文献
Bathula, Surendar Reddy; Reddy, Muktapuram Prathap; Viswanadham, K. K. Durga Rao; Sathyanarayana, Pochampalli; Reddy, Maddi Sridhar
European Journal of Organic Chemistry, 2013 , # 21 p. 4552 - 4557