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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89928-57-4
合成路线
（共 9 条）
89928-55-2
→
反应条件
89928-57-4
反应条件
thionyl chloride T=60°C; 15 h;
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
56661-74-6
→
反应条件
89928-57-4
反应条件
1: 97 percent / HCl / 3 h / Heating 2: 41 percent / 25percent ammonia / 264 h / Ambient temperature 3: 84 percent / HCl / 4 h / Heating 4: 92 percent / POCl3, PCl5 / 3 °C / Heating 5: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 6: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89928-67-6
→
反应条件
89928-57-4
反应条件
1: 41 percent / 25percent ammonia / 264 h / Ambient temperature 2: 84 percent / HCl / 4 h / Heating 3: 92 percent / POCl3, PCl5 / 3 °C / Heating 4: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 5: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89928-70-1
→
反应条件
89928-57-4
反应条件
1: 72 percent / NH3 / benzene / 1 h / Ambient temperature 2: 76.4 percent / 25percent ammonia / ethanol; H2O / 16 h / Ambient temperature 3: 99.5 percent / HCl dil. / H2O / 3.5 h / Heating 4: 84 percent / HCl / 4 h / Heating 5: 92 percent / POCl3, PCl5 / 3 °C / Heating 6: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 7: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
56661-82-6
→
反应条件
89928-57-4
反应条件
1: 84 percent / HCl / 4 h / Heating 2: 92 percent / POCl3, PCl5 / 3 °C / Heating 3: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 4: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89928-68-7
→
反应条件
89928-57-4
反应条件
1: 99.5 percent / HCl dil. / H2O / 3.5 h / Heating 2: 84 percent / HCl / 4 h / Heating 3: 92 percent / POCl3, PCl5 / 3 °C / Heating 4: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 5: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89928-69-8
→
反应条件
89928-57-4
反应条件
1: 76.4 percent / 25percent ammonia / ethanol; H2O / 16 h / Ambient temperature 2: 99.5 percent / HCl dil. / H2O / 3.5 h / Heating 3: 84 percent / HCl / 4 h / Heating 4: 92 percent / POCl3, PCl5 / 3 °C / Heating 5: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 6: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89928-78-9
→
反应条件
89928-57-4
反应条件
1: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 2: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
89929-01-1
4-甲基-1-氧代-1,2-二氢异喹啉-3-羧酸甲酯
→
反应条件
89928-57-4
反应条件
1: 92 percent / POCl3, PCl5 / 3 °C / Heating 2: 98 percent / 10percent NaCO3 / methanol; H2O / 2.5 h / Heating 3: 83 percent / thionyl chloride / 15 h / 60 °C View Scheme
参考文献
Vittorio; Santagati; Lancetta; Duro; Arrigo Reina; Cosentino
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 3 p. 217 - 228
