2-氰基-3-乙氧基-2-丁类硫代酰胺合成路线 （共 6 条）
反应条件
in water Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, # 4 p. 1093 - 1096
反应条件
1: ammonia / methanol / 20 °C 2: dihydrogen peroxide / methanol / 4 h / 0 °C / |Reflux View Scheme
参考文献
INTERMUNE, INC.; BUCKMAN, Brad, O.; NICHOLAS, John, B.; EMAYAN, Kumaraswamy; SEIWERT, Scott, D.
Patent: WO2013/25733 A1, 2013 ;
反应条件
1: 79 percent / CHCl3 / 0.33 h / Heating 2: 70 percent / 0.1N-NaOH / 80 - 85 °C / few minutes View Scheme
参考文献
Giori; Veronese; Vicentini; Guarneri
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 4 p. 1093 - 1096
反应条件
in water Ambient temperature;
参考文献
Giori; Veronese; Vicentini; Guarneri
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 4 p. 1093 - 1096
反应条件
hydrogen sulfide; triethylamine in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
INTERMUNE, INC.; BUCKMAN, Brad, O.; NICHOLAS, John, B.; EMAYAN, Kumaraswamy; SEIWERT, Scott, D.
Patent: WO2013/25733 A1, 2013 ;
Location in patent: Paragraph 0434 ;
反应条件
ammonia in methanol
T=20°C;
参考文献
INTERMUNE, INC.; BUCKMAN, Brad, O.; NICHOLAS, John, B.; EMAYAN, Kumaraswamy; SEIWERT, Scott, D.
Patent: WO2013/25733 A1, 2013 ;
Location in patent: Paragraph 0435 ;
