(4-甲基联苯-3-基)-甲醇合成路线 （共 5 条）
反应条件
potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=100°C; 15 h;
参考文献
Hatanaka, Yasuo; Fukushima, Satoshi; Hiyama, Tamejiro
Chemistry Letters, 1989 , p. 1711 - 1714
Title/Abstract Full Text Show Details
Hatanaka, Yasuo; Goda, Ken-ichi; Okahara, Yoshinori; Hiyama, Tamejiro
Tetrahedron, 1994 , vol. 50, # 28 p. 8301 - 8316
反应条件
sodium carbonate in water; N,N-dimethyl-formamide
T=90°C; Suzuki cross-coupling reaction; 0.5 h;
参考文献
Borhade, Sanjay R.; Waghmode, Suresh B.
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 310 - 319
反应条件
1: SbF3
2: 86 percent / KF / (η3-C3H5PdCl)2 / dimethylformamide / 15 h / 100 °C
View Scheme
参考文献
Hatanaka, Yasuo; Fukushima, Satoshi; Hiyama, Tamejiro
Chemistry Letters, 1989 , p. 1711 - 1714
反应条件
1: CH2Cl2 / 3 h / Ambient temperature
2: pyridine, DMAP, Et3N / CH2Cl2 / 16 h / Ambient temperature
3: 96 percent / CF3COOH / CH2Cl2 / 20 h / Ambient temperature
View Scheme
参考文献
Wendeborn, Sebastian; Berteina, Sabine; Brill, Wolfgang K.-D.; De Mesmaeker, Alain
Synlett, 1998 , # 6 p. 671 - 675
反应条件
Yield given. Multistep reaction;
参考文献
Wendeborn, Sebastian; Berteina, Sabine; Brill, Wolfgang K.-D.; De Mesmaeker, Alain
Synlett, 1998 , # 6 p. 671 - 675
