4′-(4-氯苯基)-2, 2′:6′, 2″-三联吡啶合成路线 （共 6 条）
反应条件
ammonium acetate in water
T=130°C; Kroehnke reaction; 0.266667 h; microwave irradiation;
参考文献
Tu, Shujiang; Jia, Runhong; Jiang, Bo; Zhang, Junyong; Zhang, Yan; Yao, Changsheng; Ji, Shunjun
Tetrahedron, 2007 , vol. 63, # 2 p. 381 - 388
反应条件
ammonium acetate in acetic acid
Heating;
参考文献
Mutai, Toshiki; Cheon, Jin-Dong; Arita, Shinpei; Araki, Koji
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 7 p. 1045 - 1050
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C
2: aq. NH3 / various solvent(s) / 2 h / 100 °C
View Scheme
参考文献
Winter, Andreas; Van Den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.
Synthesis, 2006 , # 17 p. 2873 - 2878
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C
2: aq. NH3 / various solvent(s) / 2 h / 100 °C
View Scheme
参考文献
Winter, Andreas; Van Den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.
Synthesis, 2006 , # 17 p. 2873 - 2878
反应条件
ammonium acetate; sodium hydroxide
1.) 180 deg C, 2 h, 2.) 120 deg C, 2 h;
参考文献
Spahni, Werner; Calzaferri, Gion
Helvetica Chimica Acta, 1984 , vol. 67, # 54 p. 450 - 454
反应条件
potassium hydroxide; sodium hydroxide; hydrogen bromide
1.) reflux; 2.) acetic acid; Yield given. Multistep reaction;
参考文献
Spahni, Werner; Calzaferri, Gion
Helvetica Chimica Acta, 1984 , vol. 67, # 54 p. 450 - 454
