4'-[4-(溴甲基)苯基]-2,2':6',2''-三联吡啶合成路线 （共 12 条）
反应条件
calcium carbonate in 1,4-dioxane; water 30 h; Reflux;
参考文献
Bhaumik, Chanchal; Das, Shyamal; Saha, Debasish; Dutta, Supriya; Baitalik, Sujoy
Inorganic Chemistry, 2010 , vol. 49, # 11 p. 5049 - 5062
反应条件
N-bromosuccinmide in benzene
HeatingIrradiation;
参考文献
Ru, Qiaorong; Xue, Zhxin; Wang, Yige; Liu, Yamei; Li, Huanrong
European Journal of Inorganic Chemistry, 2014 , # 3 p. 469 - 474
反应条件
1: 1.) CH3COONH4, CH3CONH2, 2.) Fe3+, H2O2, NaOH / 1.) reflux, 4 h
2: 85 percent / NBS, (PhCOO)2 / benzene / 18 h / Heating
View Scheme
参考文献
Bonhote, Pierre; Moser, Jacques-E.; Humphry-Baker, Robin; Vlachopoulos, Nicolas; Zakeeruddin, Shaik M.; Walder, Lorenz; Graetzel, Michael
Journal of the American Chemical Society, 1999 , vol. 121, # 6 p. 1324 - 1336
反应条件
1: sodium hydroxide / ethanol
2: methanol / Reflux
3: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane
View Scheme
参考文献
Das, Priyadip; Ghosh, Amrita; Kesharwani, Manoj K.; Ramu, Vadde; Ganguly, Bishwajit; Das, Amitava
European Journal of Inorganic Chemistry, 2011 , # 20 p. 3050 - 3058
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
2 h; Reflux;
参考文献
Romashkina; Majouga; Beloglazkina; Pichugina; Askerka; Moiseeva; Rakhimov; Zyk
Russian Chemical Bulletin, 2012 , vol. 61, # 12 p. 2265 - 2281
Izv. Akad. Nauk, Ser. Khim., 2012 , vol. 61, # 12 p. 2244 - 2260,17
反应条件
1: sodium hydroxide / triglyme (triethylene glycol dimethyl ether) / 60 °C
2: ammonium acetate / ethanol / Reflux
3: N-bromosuccinmide / benzene / Reflux
View Scheme
参考文献
Li, Dongmei; Zhang, Qiong; Wang, Peng; Wu, Jieying; Kan, Yuhe; Tian, Yupeng; Zhou, Hongping; Yang, Jiaxiang; Tao, Xutang; Jiang, Minhua
Dalton Transactions, 2011 , vol. 40, # 32 p. 8170 - 8178
反应条件
1: methanol / Reflux
2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane
View Scheme
参考文献
Das, Priyadip; Ghosh, Amrita; Kesharwani, Manoj K.; Ramu, Vadde; Ganguly, Bishwajit; Das, Amitava
European Journal of Inorganic Chemistry, 2011 , # 20 p. 3050 - 3058
反应条件
1: methanol / Reflux
2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane
View Scheme
参考文献
Das, Priyadip; Ghosh, Amrita; Kesharwani, Manoj K.; Ramu, Vadde; Ganguly, Bishwajit; Das, Amitava
European Journal of Inorganic Chemistry, 2011 , # 20 p. 3050 - 3058
反应条件
1: ammonium acetate / ethanol / Reflux
2: N-bromosuccinmide / benzene / Reflux
View Scheme
参考文献
Li, Dongmei; Zhang, Qiong; Wang, Peng; Wu, Jieying; Kan, Yuhe; Tian, Yupeng; Zhou, Hongping; Yang, Jiaxiang; Tao, Xutang; Jiang, Minhua
Dalton Transactions, 2011 , vol. 40, # 32 p. 8170 - 8178
反应条件
1: potassium hydroxide; ammonium hydroxide / ethanol / 12 h / 20 °C
2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 2 h / |Reflux
View Scheme
参考文献
Romashkina; Majouga; Beloglazkina; Pichugina; Askerka; Moiseeva; Rakhimov; Zyk
Russian Chemical Bulletin, 2012 , vol. 61, # 12 p. 2265 - 2281
Izv. Akad. Nauk, Ser. Khim., 2012 , vol. 61, # 12 p. 2244 - 2260,17
