反应条件
1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C
1.2: glacial acetic acid / tetrahydrofuran / -78 °C
2.1: sodium acetate / tetrahydrofuran / 20 °C
3.1: 65 percent / hydrogen peroxide; lithium hydroxide / tetrahydrofuran; H2O / 0 - 20 °C
4.1: 96 percent / hydrogen; acetic acid / Pd/C / H2O / 18 h
View Scheme
参考文献
Ku, Hui-Young; Jung, Junyang; Kim, Soo-Hyun; Kim, Hee Yeon; Ahn, Kyo Han; Kim, Sung-Gon
Tetrahedron Asymmetry, 2006 , vol. 17, # 7 p. 1111 - 1115
